| Energy Dispersive X-ray Spectroscopy
(EDS), also referred to as EDX, is a technique used
in conjunction with Scanning Electron Microscopy (SEM)
. First the area of interest is identified through SEM
imaging. X-rays generated by the SEM’s focused
electron beam are then collected by the EDS detector
where the energy of the X-ray is determined. The number
of X-rays are counted for each particular energy and
displayed on a graph of counts vs. energy. Since each
element releases X-rays with unique energy signatures
it is possible to identify the parent atoms from the
X-ray spectrum. All elements greater than Beryllium
(Be) can generally be detected and quantitative analysis
is possible. Element distribution mapping is another
useful technique using EDS. During element mapping,
one or more X-ray energies corresponding to one or more
elements are collected as the SEM scans the electron
beam over a selected area. The X-ray data is synchronized
with the SEM image and an ‘element image’
is created showing the presence of the selected element
throughout the selected area. This can be a powerful
tool for determining the distribution of a contaminant
or the structure of a sample.
|
|
 |